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Chem 337 Syllabus, Fall, 2009


Course CHEM 337 Practical Organic Chemistry I
 

Section 001

MW, 1:40-4:20, SENG A402
  Section 002 MW, 4:30-7:05, SENG A402
  Section 003 TR, 1:40-4:20, SENG A402
 
Instructors John Balyeat, Eng 245, 255-3852, jbalyeat@uccs.edu
     Office hours: Monday-Thursday, 11:00-12:30
Tisha Mendiola: tmendiol@uccs.edu
 

Materials:
  1. Microscale and Miniscale Organic Chemistry Laboratory Experiments, 2nd Edition, Schoffstall, Gaddis & Druelinger, McGraw-Hill, 2004.

  2. Student Lab Notebook with spiral binding, carbonless (Hayden-McNeil, ISBN 978-1-930882-74-2 or ISBN 978-930882-74-8)

  3. Safety goggles, lab apron, and nitrile gloves


Goals for the Course

This course integrates and complements the material you will learn in lecture and helps prepare you to study more advanced topics, such as biochemistry. This course will:

  1. Provide an active-learning environment that illustrates the reactions, principles, and theories learned in lecture.

  2. Help you develop scientific inquiry skills, such as hypothesis generation, observation, description, data manipulation, and evaluation of results.

  3. Help your learn basic laboratory notebook skills.

  4. Help you develop laboratory technical skills.

  5. Provide experience using scientific instrumentation.

  6. Improve you problem-solving skills through collaborative and individual reflection and analysis.

  7. Provide opportunities to use chemical reference materials, the goal of which is to use and dispose of chemicals in a safe, approved manner.


Successful Lab Experiences

Being a successful organic chemistry student involves

  • being prepared for the laboratory,

  • being observant,

  • understanding what you are doing and why you are doing it,

  • developing careful and methodical laboratory technique,

  • interpreting results appropriately,

  • being able to summarize and analyze the results accordingly.

To be successful, several steps in the experimental process are essential. These are:

  • Before coming to lab ...

  1. Read the entire exercise or experiment.

  2. Prepare lab notebook.

  3. Do pre-lab assignment/questions in lab text (where applicable).

  • In lab ...

  1. Perform exercise or experiment.

  2. Record all data and observations directly in notebook.

  • By the start of the next lab ...

  1. Complete all necessary calculations in lab notebook.

  2. Submit typed lab report or datasheet with carbon copies of notebook pages, TLC plates, spectra, etc., attached.


Exams

Midterm exams, quizzes, a lab practical, and/or a final exam will be administered. See the grading section of this syllabus or the lab schedule web page for specifics.  Nomographs, spectral tables, etc., will be provided as needed.


Safety

  • Safety Test - You must pass the safety test by Sep 8, to continue doing lab work. Review material and the actual test are available in the "Prelab Quizzes" section of WebCT.

  • Pregnancy - Women who are pregnant of who become pregnant during the semester MUST have written approval from the Student Health Service to continue in the class. Submit a copy or the approval paperwork to the course instructor.

  • Chronic illness - Students who have a chronic illness MUST have written approval from the Student Health Service to continue in the class. Submit a copy or the approval paperwork to the course instructor.


The Laboratory Notebook

For those of you whose intent is to become a scientist, doctor, or health science professional, it is essential to know how to keep a clear, accurate record of your work. In this course, you will learn the basics of keeping a laboratory notebook.

Your chemistry laboratory notebook documents everything you do with respect to a given laboratory experiment. From pre-lab preparation to observations to calculations to final conclusions, it should all be recorded your lab notebook. It should be detailed enough such that another chemist could successfully repeat your work and obtain comparable results.

You will undoubtedly discover that keeping a good lab notebook is a lot of work. There is great attention given to detail and prescribed formats. So much so that you may question the necessity of it all. But for now you'll just have to trust us. It's important. In fact, in the scientific academic and professional arenas, the lab notebook is a legal document, often signed each day by the scientist and a knowledgeable witness. Although we won't be taking it to that extreme, you do need to accord the notebook its due significance and give it the time and attention it deserves.

You must have certain portions of your notebook prepared before coming to lab. If you forget your notebook, you will need to go get it before starting lab. If your laboratory notebook is not sufficiently prepared in the estimation of your instructor, as a minimum you will lose a significant amount of points for the experiment. Worst case, you will not be allowed to perform the lab, resulting in a score of zero. When you actually perform the experiment, you will not have your lab text to rely on. What you will have is what you prepared beforehand in your notebook.

Lab notebooks may be used during the midterms exams. So keeping a good notebook is also advantageous in this regard.

For details about maintaining your lab notebook, click on this link.  For an example, click here.
 


Lab Reports

  • A formatted report form or datasheet is provided for most experiments. These datasheets will generally be typed.

  • You will be required to enter molecular structures using a chemical software drawing program such as ChemSketch, ChemDraw, or Chem3D.

  • These programs are installed on the computers in SCI 242. A free download of ChemSketch is available at http://www.acdlabs.com.  (PC only).

  • Datasheets forms are usually linked to the experiments on the schedule web page. Some datasheets will be handed out during the lab.


Late Lab Report Policy

  • Completed laboratory reports or datasheets are due one week after completion of the experiment unless directed otherwise.

  • Reports and datasheets are due at the beginning of the lab period.

  • Ten percentage points per weekday will be deducted from reports or datasheets that are turned in late.

  • Reports or datasheets that are turned in on the scheduled day but after the start of the lab period will receive a five percentage point deduction.

  • Lab reports or datasheets that are more than a week late will receive a zero score.

  • Failure to turn in three reports will result in a failing grade for the course.


Missed Lab Policy

  • You are expected to be present, on time, and prepared for each laboratory meeting.

  • If you miss a lab because of illness or emergency, contact the lab instructor, John Balyeat, at 255-3852 and send an email.

  • Missed labs can NOT be made up. Accommodation will be made only with the prior approval of the lab instructor and ONLY in case of emergency, certified illness, death in the family, etc. To obtain approval to miss a lab, present a completed Missed Lab Form and documentation explaining why you missed the lab to your lab instructor. Click to download the Missed Lab Form. Vacations and family trips are not acceptable reasons for missing labs.
  • Approval will not be given for more than 2 missed labs. Subsequent missed labs will receive a zero.
  • Missed labs labs will receive the class section average for that lab.
  • If you are more than 30 minutes late to lab you will not be allowed to perform the experiment. It will be recorded as an unexcused absence.

  • Unexcused absences will result in a score of zero for that lab.

  • Three unexcused absences will result in a failing grade for the course.

  • Missing lab to study for another course is not a reasonable excuse. Plan ahead.

  • If you know a head of time you will miss a lab, inform your instructor and make arrangements to do the lab at an alternative time.


Academic Policies

  • From UCCS's Academic Principles:   

"Students, as responsible members of the academic community, are obligated to maintain basic standards of integrity, and are expected to take an active role in encouraging other members to respect these standards. If students suspect a violation has been committed, they a responsibility to discuss their suspicion with a member of the faculty or university administration. Students should make themselves familiar with the basic tenets of the Honor Code." (1)

"Faculty members have the responsibility to preserve and transmit academic values in the learning environment and in the example they provide to students. To this end, they are expected to instill in their students a respect for integrity and a desire to behave honestly; they must also take measures to discourage student academic dishonesty. To meet these responsibilities, faculty members must follow the policies and procedures stated in the UCCS Academic Honor Code." (1)

  • "The essence of science is the pursuit and transmission of knowledge, an endeavor that depends upon honesty, objectivity, intellectual freedom, and trust over generations, across disciplines, and across national borders. As every researcher depends on the validity of others' previous work, and because no single individual can master every dimension of any field, the practical demands of science reinforce an inherently moral social contract among researchers"— from "The Ethical Dimensions of the Biological Sciences"(2).

     
  • Conduct your affairs with integrity and all will be well. Translation: all work submitted must be your own. Work that is copied from another student will receive no credit (for either student).  The determination of academic misconduct will be made by the lab instructor and lab lecturer. Depending upon the infraction, sanctions may range from partial or total loss of points to a failing grade in the class. All infractions are reported to the department head / LAS dean as appropriate. Additionally, the student may be referred for disciplinary action. Clearly, it's not worth it.  For more information about forms of academic dishonesty, click on this link. (Covers plagiarism, cheating, fabrication and falsification, and complicity in academic dishonesty.)
     

  • Specific application of honor and integrity to organic chemistry laboratories (adapted from the Policy on Scientific Integrity (3), College of Charleston, Charleston, SC).

Keep an open, objective mind while carrying out your lab experiments. If the expected outcome is not obtained, there is a reasonable, logical explanation.

Carry out your own experiments. If you require assistance, ask your instructor.

Report your findings accurately. Do not embellish, alter or ignore data.

Following the lab, it is acceptable and encouraged to engage other lab participants in a general discussion of results and understanding of the laboratory principles.

When it is time to write your report, do this by yourself. Work independently when deriving your conclusions. Complete the datasheet/report without the assistance of other students. If you get stuck, see your instructor for help.

When asked to provide printed chemical structures, do not cut and paste from the web. Draw them with ChemSketch, ChemDraw, or other commercially available software.

Cite materials used as directed by your instructor.

Acknowledge, in writing, those who provided assisted in pre- or post-lab understanding of the material.

  • The following are examples of academic misconduct we will not tolerate. (3).

    • Modifying data to conform to an expected outcome
    • Copying another student's data into your own notebook or report
    • Using another student's interpretation and presenting it as your own
    • Copying previously interpreted data or graded reports from this lab course
    • Providing your data or graded lab reports to another student who presents it as their own
    • Presenting data collected in prior semesters for credit in the present semester

     

  • Scores and grades will be posted on WebCT.

(1) http://www.uccs.edu/~dos/studentconduct/academicprinciples.html, accessed Aug 12, 2009

(2) The Roots of Honor and Integrity in Science. Cambridge University Press: Cambridge, U.K.; Bulger, R.E.; Heitman, E.: Reiser, S.J.; 1993; p. 41.

(3) http://spinner.cofc.edu/~chem/advising/integrity.html?referrer=webcluster&, accessed Aug 17, 2009.

 


Grading and Course Percentages

Activity Total
19 Datasheets @ 50 each 950
3 Midterm Exams @ 100 each 300
1 Lab Practical @ 100 100
TOTAL 1350

 

Grading Scale

90.0% A
80.0% B
70.0% C
60.0% D
<60.0% F

 


Cell Phones and MP3 Players

No cell phones will be allowed in lecture or lab. Please keep them in your backpack or jacket on "silent". Ditto for MP3 players and other similar non-academic electronic devices.


Disabilities

If you have a disability for which you are requesting an accommodation, you are encouraged to contact Disability Services within the first week of classes. Contact information: Main Hall, Room 105, 719-262-3354, dservice@uccs.edu


Questions or Comments? Contact John Balyeat