Microscale and Miniscale Organic Chemistry Laboratory Experiments, 2nd Edition


 
Table of Contents
 
Preface xxi
Walkthrough xxvi
Introduction 1
Chapter One Techniques in the Organic Chemistry Laboratory 9
Chapter Two Spectroscopic Methods and Molecular Modeling 109
Chapter Three Applications Using Laboratory Resources and Techniques 183
Chapter Four Alcohols and Alkyl Halides 221
Chapter Five Synthesis of Alkenes 229
Chapter Six Alkene Addition Reactions 237
Chapter Seven Stereochemistry 255
Chapter Eight Introduction to Nucleophilic Substitution Reactions 261
Chapter Nine Dienes and Conjugation 271
Chapter Ten Qualitative Organic Analysis I 281
Chapter Eleven Reactions of Aromatic Side Chains 290
Chapter Twelve Electrophilic Aromatic Substitution 298
Chapter Thirteen Combined Spectroscopy and Advanced Spectroscopy 323
Chapter Fourteen Organometallics 351
Chapter Fifteen Alcohols and Diols 364
Chapter Sixteen Ethers 376
Chapter Seventeen Aldehydes and Ketones 385
Chapter Eighteen Enols, Enolates and Enones 404
Chapter Nineteen Carboxylic Acids 419
Chapter Twenty Carboxylic Acid Esterss 430
Chapter Twenty-One Dicarbonyl Compounds 441
Chapter Twenty-Two Amines 450
Chapter Twenty-Three Aryl Halides 475
Chapter Twenty-Four Phenols 480
Chapter Twenty-Five Carbohydrates 489
Chapter Twenty-Six Lipids 407
Chapter Twenty-Seven Amino Acids and Derivatives 518
Chapter Twenty-Eight Qualitative Organic Analysis II 529
Chapter Twenty-Nine Projects 578
Appendix A Tables of Derivatives for Qualitative Organic Analysis 627
Appendix B Laboratory Skills and Calculations 632
Appendix C Designing a Flow Scheme 637
Appendix D Material Safety Data Sheet 639
Appendix E Tables of Common Organic Solvents and Inorganic Solutions 643
Index 645

 

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